2,3-Dinitrophenol → Sodium dinitrophenolate

HRID 874859

Reaktionsgleichung

Reaktionsgleichung von HRID 874859
[N+:1]([C:4]1[C:5]([N+:11]([O-:13])=[O:12])=[C:6]([OH:10])[CH:7]=[CH:8][CH:9]=1)([O-:3])=[O:2].[H-].[Na+:15]>C1COCC1>[N+:1]([C:4]1[C:5]([N+:11]([O-:13])=[O:12])=[C:6]([O-:10])[CH:7]=[CH:8][CH:9]=1)([O-:3])=[O:2].[Na+:15]

Komponenten

4

Edukt 2

HCID 61912,3-DinitrophenolHCID 24758Sodium hydride

Produkt 1

HCID 86649331Sodium dinitrophenolate

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 8028TetrahydrofuranLösungsmittel

Versuchsvorschrift

The anhydrous dinitrophenol (10.0 g, 54.3 mmol) was dissolved in anhydrous THF (300 mL) and then NaH(1.30 g, 54.3 mmol) was added slowly. After the solution was stirred for 3 hrs, solvent was removed under the reduced pressure to obtain 100 mol % sodium dinitrophenolate.

Aufarbeitung

  1. customsolvent was removed under the reduced pressure

Quellen und Nachweise

ORD-Eintrag
ord-d8af27706dff4fbb87b4281472467d2c
Quelldatensatz
uspto-grants-2015_03
Patentnummer
US08981043B2

Verknüpfte Notizen

Wird geladen…