2,3-Dinitrophenol → Sodium dinitrophenolate

HRID 877867

Reaktionsgleichung

Reaktionsgleichung von HRID 877867
[N+:1]([C:4]1[C:5]([N+:11]([O-:13])=[O:12])=[C:6]([OH:10])[CH:7]=[CH:8][CH:9]=1)([O-:3])=[O:2].[H-].[Na+:15]>C1COCC1>[N+:1]([C:4]1[C:5]([N+:11]([O-:13])=[O:12])=[C:6]([O-:10])[CH:7]=[CH:8][CH:9]=1)([O-:3])=[O:2].[Na+:15]

Komponenten

4

Edukt 2

HCID 61912,3-DinitrophenolHCID 24758Sodium hydride

Produkt 1

HCID 86649331Sodium dinitrophenolate

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 8028TetrahydrofuranLösungsmittel

Versuchsvorschrift

The anhydrous dinitrophenol (10.0 g, 54.3 mmol) was dissolved in anhydrous THF (300 mL) and then NaH (1.30 g, 54.3 mmol) was added slowly. After the solution was stirred for 3 hrs, solvent was removed under the reduced pressure to obtain 100 mol % sodium dinitrophenolate.

Aufarbeitung

  1. customsolvent was removed under the reduced pressure

Quellen und Nachweise

ORD-Eintrag
ord-bb64b922e5af466a87709b09e9ad12cb
Quelldatensatz
uspto-grants-2015_03
Patentnummer
US08987411B2

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