Benzyl 2-(2-(methylcarbamoyl)morpholino)acetate → HCID 66760446, Verbindung
Reaktionsgleichung
[CH3:1][NH:2][C:3]([CH:5]1[CH2:10][N:9]([CH2:11][C:12]([O:14]CC2C=CC=CC=2)=[O:13])[CH2:8][CH2:7][O:6]1)=[O:4]>C(O)C.[Pd]>[CH3:1][NH:2][C:3]([CH:5]1[CH2:10][N:9]([CH2:11][C:12]([OH:14])=[O:13])[CH2:8][CH2:7][O:6]1)=[O:4]Komponenten
4
Edukt 1
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 2
Versuchsvorschrift
benzyl 2-(2-(methylcarbamoyl)morpholino)acetate was dissolved in ethanol (40 mL), Pd/C 10% (100 mg) was added to the solution, and the mixture was stirred overnight under hydrogen (balloon) then filtered through celite and concentrated to give 2-(2-(methylcarbamoyl)morpholino)acetic acid. MS (APCI) 203 (M+1)
Aufarbeitung
- filtrationthen filtered through celite and
- concentrationconcentrated
Quellen und Nachweise
- ORD-Eintrag
- ord-d936177f550e403ab7f5393bfef6e89a
- Quelldatensatz
- uspto-grants-2012_08
- Patentnummer
- US08252793B2
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