Ethanol → HCID 23338142, Verbindung

HRID 903321

Reaktionsgleichung

Reaktionsgleichung von HRID 903321
[Na].ClC1N=NN=C(Cl)C=1.[Cl:10][C:11]1[N:16]=[C:15](Cl)[N:14]=[C:13]([N:18]([CH3:20])[CH3:19])[N:12]=1.[CH2:21]([OH:23])[CH3:22]>>[Cl:10][C:11]1[N:16]=[C:15]([O:23][CH2:21][CH3:22])[N:14]=[C:13]([N:18]([CH3:20])[CH3:19])[N:12]=1

Komponenten

5

Edukt 4

HCID 702Ethanol2×HCID 169852,4-Dichloro-6-(dimethylamino)-1,3,5-triazineHCID 5360545SodiumHCID 18348308HCID 18348308, Verbindung

Produkt 1

HCID 23338142HCID 23338142, Verbindung

Versuchsvorschrift

A solution of sodium (0.46 g.) in ethanol (50 ml.) was added with stirring and waterbath cooling (25° C.) to a solution of the dichlorotriazine (3.86 g.) from (a) in ethanol (50 ml.). Following the addition the solution was poured into ice water (250 ml.) and the product collected, dried and crystallised from petroleum as needles (2.5 g.) having a melting point of 124° C.

Aufarbeitung

  1. additionthe addition the solution
  2. customthe product collected
  3. customdried
  4. customcrystallised from petroleum as needles (2.5 g.)

Quellen und Nachweise

ORD-Eintrag
ord-66b37f85eaa14fb1b300dbb4ab41495e
Quelldatensatz
uspto-grants-1980_10
Patentnummer
US04226990

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