Acetone → HCID 70525545, Verbindung

HRID 905092

Reaktionsgleichung

Reaktionsgleichung von HRID 905092
[C:1]([C:6]1[CH:11]=[C:10]([C:12]([CH2:15][CH3:16])([CH3:14])[CH3:13])[CH:9]=[CH:8][C:7]=1O)([CH2:4][CH3:5])([CH3:3])[CH3:2].[CH2:18](Br)[CH:19]=[CH2:20].[C:22](=[O:25])([O-])[O-].[CH3:26][C:27]([CH3:29])=O>>[C:1]([C:6]1[CH:11]=[C:10]([C:12]([CH2:15][CH3:16])([CH3:14])[CH3:13])[CH:9]=[CH:8][C:7]=1[CH:20]=[CH:19][CH2:18][O:25][CH2:22][CH:26]=[CH:27][C:29]1[CH:8]=[CH:7][C:6]([C:1]([CH2:4][CH3:5])([CH3:3])[CH3:2])=[CH:11][C:10]=1[C:12]([CH2:15][CH3:16])([CH3:14])[CH3:13])([CH2:4][CH3:5])([CH3:3])[CH3:2]

Komponenten

5

Edukt 4

HCID 180AcetoneHCID 7841Allyl bromideHCID 84552,4-Di-tert-pentylphenolHCID 19660Carbonate Ion

Produkt 1

HCID 70525545HCID 70525545, Verbindung

Versuchsvorschrift

117.2 g of 2,4-di-t-amylphenol and 90.7 g of allylbromide was dissolved in 500 ml of acetone. Thereto was added 103.5 g of pottassium carbonate and refluxed in a water bath for 20 hours. Then reaction mixture was filtered under suction and filtration residue was rinsed with 100 ml of acetone, thereafter this was again mixed with the mother solution and then under reduced pressure acetone and excess allyl bromide was distilled out.

Aufarbeitung

  1. temperaturerefluxed in a water bath for 20 hours
  2. customThen reaction mixture
  3. filtrationwas filtered under suction and filtration residue
  4. washwas rinsed with 100 ml of acetone
  5. additionthis was again mixed with the mother solution
  6. distillationunder reduced pressure acetone and excess allyl bromide was distilled out

Quellen und Nachweise

ORD-Eintrag
ord-6ce65696a38043df969eb3d936abe02e
Quelldatensatz
uspto-grants-1983_12
Patentnummer
US04421846

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