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Sodium Thiosulfate → HCID 22248470, Verbindung

HRID 914916
Notizen
Druckvorschau

Reaktionsgleichung

Reaktionsgleichung von HRID 914916
[F:1][C:2]1[CH:23]=[CH:22][CH:21]=[CH:20][C:3]=1[CH2:4][S:5][CH:6]1[CH2:11][CH2:10][N:9]([CH2:12][C:13]2[C:14](=[O:19])[NH:15][CH:16]=[CH:17][N:18]=2)[CH2:8][CH2:7]1.ClC1C=CC=C(C(OO)=[O:32])C=1.S([O-])([O-])(=O)=S.[Na+].[Na+]>ClCCl>[F:1][C:2]1[CH:23]=[CH:22][CH:21]=[CH:20][C:3]=1[CH2:4][S:5]([CH:6]1[CH2:7][CH2:8][N:9]([CH2:12][C:13]2[C:14](=[O:19])[NH:15][CH:16]=[CH:17][N:18]=2)[CH2:10][CH2:11]1)=[O:32]
KomponentenVersuchsvorschriftAufarbeitungQuellen und NachweiseNotizen zur Reaktion

Komponenten

5

Edukt 3

HCID 24477Sodium ThiosulfateHCID 70297m-Chloroperbenzoic acid2×HCID 222485193-(4-(2-fluorobenzylthio)piperidino]methyl-1H-pyrazin-2-one

Produkt 1

HCID 22248470HCID 22248470, VerbindungAusbeute 27 %

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 6344DichloromethaneLösungsmittel2×

Versuchsvorschrift

After dissolving 57 mg of 3-[4-(2-fluorobenzylthio)piperidino]methyl-1H-pyrazin-2-one in 3 ml of dichloromethane, 31 mg of 3-chloroperbenzoic acid was added at below −70° C., the mixture was stirred for 30 minutes, and then an additional 5 mg of 3-chloroperbenzoic acid was added and the stirring was continued for 20 minutes. Aqueous sodium thiosulfate solution was added to the reaction solution and extraction was performed with dichloromethane. The organic layer was washed with saturated brine and dried over anhydrous magnesium sulfate, and then the solvent was distilled off under reduced pressure. The residue was purified by silica gel column chromatography (solvent: chloroform/methanol/ammonia water) to obtain the title compound (16 mg, 27% yield).

Aufarbeitung

  1. additionwas added at below −70° C.
  2. waitthe stirring was continued for 20 minutes
  3. washThe organic layer was washed with saturated brine
  4. dry with materialdried over anhydrous magnesium sulfate
  5. distillationthe solvent was distilled off under reduced pressure
  6. customThe residue was purified by silica gel column chromatography (solvent: chloroform/methanol/ammonia water)

Quellen und Nachweise

ORD-Eintrag
ord-c0e09161955b47bd83565e7941dcdbbf
Quelldatensatz
uspto-grants-2007_09
DOI
10.6084/m9.figshare.5104873.v1
Patentnummer
US07265108B2

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