HCID 69229653, Verbindung → HCID 11351366, Verbindung
Reaktionsgleichung
[NH2:1][C:2]1[CH:3]=[C:4]2[C:8](=[CH:9][CH:10]=1)[N:7]([CH2:11][C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1)[C:6]([C:18]([O:20]CC)=[O:19])=[C:5]2[C:23]1[CH:28]=[CH:27][C:26]([C:29]([CH3:32])([CH3:31])[CH3:30])=[CH:25][CH:24]=1>O>[CH2:11]([N:7]1[C:8]2[C:4](=[CH:3][C:2]([N:1]3[CH:9]=[CH:10][CH:2]=[CH:3]3)=[CH:10][CH:9]=2)[C:5]([C:23]2[CH:24]=[CH:25][C:26]([C:29]([CH3:31])([CH3:30])[CH3:32])=[CH:27][CH:28]=2)=[C:6]1[C:18]([OH:20])=[O:19])[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1Komponenten
3
Reagenzien, Katalysatoren, Lösungsmittel 1
Versuchsvorschrift
The title compound was prepared from ethyl 5-amino-1-benzyl-3-(4-tert-butylphenyl)-1H-indole-2-carboxylate followed the procedures of Example 1 Step 3 and Step 4 as a beige solid: 1H NMR (DMSO-d6) δ 1.35 (s, 9 H), 5.86 (s, 2 H), 6.21 (s, 2 H), 7.05-7.85 (m, 14 H); MS (ESI) m/z 447 ([M-H]−); HRMS calcd for C30H29N2O2: 449.2230; found (ESI+) 449.2225; Anal. calcd for C30 H28N2O2.0.2 H2O: C, 79.69; H, 6.33; N, 6.20. Found: C, 79.70; H, 6.18; N, 6.20.
Quellen und Nachweise
- ORD-Eintrag
- ord-438d3c8fa6b94f72aae8da2cc67ac484
- Quelldatensatz