Ethanol → HCID 58081363, Verbindung

HRID 928356

Reaktionsgleichung

Reaktionsgleichung von HRID 928356
[CH2:1]([O:3][C:4](=[O:10])[C:5](OCC)=[NH:6])[CH3:2].[C:11]1([CH2:17][C:18]([NH:20][NH2:21])=O)[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1.[CH2:22](O)[CH3:23]>>[CH2:1]([O:3][C:4]([C:5]1[N:6]=[C:18]([CH2:17][C:11]2[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=2)[NH:20][N:21]=1)=[O:10])[CH2:2][CH2:22][CH3:23]

Komponenten

4

Edukt 3

HCID 702EthanolHCID 70301Benzeneacetic acid, hydrazideHCID 10920638Ethyl 2-ethoxy-2-iminoacetate

Produkt 1

HCID 58081363HCID 58081363, Verbindung

Reaktionsbedingungen

Temperatur
80 °C

Versuchsvorschrift

Ethyl-2-ethoxy-2-iminoacetate (1.318 g, 9.08 mmol) and phenyl acetic acid hydrazide (1.364 g, 9.08 mmol) were mixed together in ethanol (20 ml) and stirred at 80° C. for 1 h. Ethanol was evaporated. The residue was dissolved in n-butanol (20 ml). The reaction mixture was stirred at 150° C. for 20 h, then solvents were evaporated.

Aufarbeitung

  1. customEthanol was evaporated
  2. dissolutionThe residue was dissolved in n-butanol (20 ml)
  3. stirringThe reaction mixture was stirred at 150° C. for 20 h
  4. customsolvents were evaporated

Quellen und Nachweise

ORD-Eintrag
ord-12d0f595110f482ea4f4751a12afcd85
Quelldatensatz
uspto-grants-2016_03
Patentnummer
US09290485B2

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