Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Ethanol | HCID 702 | — |
| Edukt | Benzeneacetic acid, hydrazide | HCID 70301 | — |
| Edukt | Ethyl 2-ethoxy-2-iminoacetate | HCID 10920638 | — |
| Produkt | HCID 58081363 | HCID 58081363 | — |
Reaktionsschritte
Ethyl-2-ethoxy-2-iminoacetate (1.318 g, 9.08 mmol) and phenyl acetic acid hydrazide (1.364 g, 9.08 mmol) were mixed together in ethanol (20 ml) and stirred at 80° C. for 1 h. Ethanol was evaporated. The residue was dissolved in n-butanol (20 ml). The reaction mixture was stirred at 150° C. for 20 h, then solvents were evaporated.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patentnummer | US09290485B2 |
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| Quelldatensatz | uspto-grants-2016_03 |
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| ORD ID | ord-12d0f595110f482ea4f4751a12afcd85 |
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| Quellennotiz | uspto-grants-2016_03 |
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