反应详情

温度

80 °C

Ethyl-2-ethoxy-2-iminoacetate (1.318 g, 9.08 mmol) and phenyl acetic acid hydrazide (1.364 g, 9.08 mmol) were mixed together in ethanol (20 ml) and stirred at 80° C. for 1 h. Ethanol was evaporated. The residue was dissolved in n-butanol (20 ml). The reaction mixture was stirred at 150° C. for 20 h, then solvents were evaporated.

1. customEthanol was evaporated
2. dissolutionThe residue was dissolved in n-butanol (20 ml)
3. stirringThe reaction mixture was stirred at 150° C. for 20 h
4. customsolvents were evaporated