Carbon Dioxide → HCID 54358079, Verbindung

HRID 965320Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 965320
[CH2:1]([O:3][C:4](=[O:37])[C:5](=[NH:36])[CH:6](P(C1C=CC=CC=1)(C1C=CC=CC=1)C1C=CC=CC=1)[CH2:7][CH2:8][NH:9][C:10]([O:12][C:13]([CH3:16])([CH3:15])[CH3:14])=[O:11])[CH3:2].[C:38](=O)=[O:39]>>[CH2:1]([O:3][C:4](=[O:37])[CH:5]([N:36]=[C:38]=[O:39])[CH2:6][CH2:7][CH2:8][NH:9][C:10]([O:12][C:13]([CH3:14])([CH3:15])[CH3:16])=[O:11])[CH3:2]

Komponenten

3

Edukt 2

HCID 280Carbon DioxideHCID 178472716HCID 178472716, Verbindung

Produkt 1

HCID 54358079HCID 54358079, Verbindung

Reaktionsbedingungen

Temperatur
50 °C

Versuchsvorschrift

The reaction solution from Example 9 is placed in a Parr® bomb and carbon dioxide (22 g, 0.5 mol) is condensed into the bomb. The bomb is sealed and heated to 50° C. for 12 hours. The bomb is cooled and vented to atmospheric pressure. The solution is transferred from the bomb to a flask and used as is in the next reaction (Example 11).

Aufarbeitung

  1. customcondensed into the bomb
  2. customThe bomb is sealed
  3. temperatureThe bomb is cooled
  4. customThe solution is transferred from the bomb to a flask
  5. customas is in the next reaction (Example 11)

Quellen und Nachweise

ORD-Eintrag
ord-4aea66748c58497d8c3f804e2902be7e
Quelldatensatz
uspto-grants-1998_06
Patentnummer
US05773571

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