Methyl-5-norbornene-2,3-dicarboxylic anhydride → Epoxy-styrene

HRID 971501

Reaktionsgleichung

Reaktionsgleichung von HRID 971501
C[C:2]12[CH:8]3[C:9]([O:11][C:12](=O)[CH:7]3[CH:4]([CH:5]=[CH:6]1)C2)=O>CC(OOC(=O)C1C=CC=CC=1)(CCC(C)(OOC(=O)C1C=CC=CC=1)C)C>[O:11]1[C:12]([C:7]2[CH:4]=[CH:5][CH:6]=[CH:2][CH:8]=2)=[CH:9]1

Komponenten

3

Edukt 1

HCID 32802Methyl-5-norbornene-2,3-dicarboxylic anhydride

Produkt 1

HCID 14299145Epoxy-styrene

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 757962,5-Dimethyl-2,5-DI-(benzoylperoxy)hexaneKatalysator

Versuchsvorschrift

To this inhibited epoxy diester-styrene mixture 5.49 parts of NADIC methyl anhydride, 0.048 part of 2,5-dimethyl-2,5 bis(benzoyl peroxy) hexane catalyst (sold by Wallace & Tierman Inc. under the tradename of Luperox 118), and 0.05 part of zinc ethyl hexoate catalyst were added, at 25° C., to provide the solventless epoxy-styrene varnish. The viscosity of the epoxy-styrene resin was measured to be about 200 cps at 25° C.

Quellen und Nachweise

ORD-Eintrag
ord-b0a3b8ccd73b4a13b4b0597aef474c94
Quelldatensatz
uspto-grants-1979_07
Patentnummer
US04160178

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