HCID 20201103, Verbindung → 4-Methyl-2-(methylthio)thiophen-3-amine
Reaktionsgleichung
[CH3:1][S:2][C:3]1[S:4][CH:5]=[C:6]([CH3:11])[C:7]=1[N+:8]([O-])=O>C(OCC)C>[CH3:1][S:2][C:3]1[S:4][CH:5]=[C:6]([CH3:11])[C:7]=1[NH2:8]Komponenten
3
Edukt 1
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 1
Versuchsvorschrift
6 g (0.22 gram atoms) freshly prepared aluminium amalgam are added over a period of about two minutes to 18.9 g (0.1 mol) of 2-methylthio-4-methyl-3-nitrothiophene dissolved in 200 ml of moist diethylether. The vigorous reaction which sets in after 5-10 minutes is kept under control by cooling the flask in ice.
Aufarbeitung
- customThe vigorous reaction which
- customafter 5-10 minutes
- temperatureby cooling the flask in ice
Quellen und Nachweise
- ORD-Eintrag
- ord-dfa6b5a73c394992a319395e4b4c1656
- Quelldatensatz
- uspto-grants-1987_05
- Patentnummer
- US04666502
Notizen zur Reaktion
Wird geladen…