Glycine → N-(1-Oxodecyl)glycine

HRID 979748Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 979748
[C:1]([Cl:12])(=[O:11])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10].[NH2:13][CH2:14][C:15]([OH:17])=[O:16]>>[C:1]([Cl:12])(=[O:11])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10].[NH2:13][CH2:14][C:15]([OH:17])=[O:16].[C:1]([NH:13][CH2:14][C:15]([OH:17])=[O:16])(=[O:11])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10]

Komponenten

5

Edukt 2

HCID 750GlycineHCID 66982Decanoyl chloride

Produkt 3

HCID 750GlycineHCID 66982Decanoyl chlorideHCID 1712391N-(1-Oxodecyl)glycineAusbeute 94 %

Versuchsvorschrift

N-Decanoylglycine was prepared by reaction of decanoyl chloride with glycine according to the procedure described in Example I. From 47.7 g (0.25 mol) of decanoyl chloride and 18.8 g (0.25 mol) of glycine was obtained 54.1 g (94%) of N-decanoylglycine, mp 104°-108° C.

Quellen und Nachweise

ORD-Eintrag
ord-0eb27852a82d4d72adeebc6964bdc46c
Quelldatensatz
uspto-grants-1987_01
Patentnummer
US04634551

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