Water → HCID 6410643, Verbindung

HRID 985938Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 985938
Cl[C:2]1[N:3]=[N:4][C:5]([C:9]2[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=2)=[CH:6][C:7]=1[CH3:8].[CH3:15][O:16][CH2:17][CH2:18][NH2:19].O>C(O)CCC>[CH3:15][O:16][CH2:17][CH2:18][NH:19][C:2]1[N:3]=[N:4][C:5]([C:9]2[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=2)=[CH:6][C:7]=1[CH3:8]

Komponenten

5

Edukt 3

HCID 962WaterHCID 80182-MethoxyethylamineHCID 1199993-Chloro-4-methyl-6-phenylpyridazine

Produkt 1

HCID 6410643HCID 6410643, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 2631-ButanolLösungsmittel

Versuchsvorschrift

A mixture of 7 g of 3-chloro 4-methyl 6-phenyl pyridazine and 7 g of 2-methoxy ethylamine in 50 ml of butanol is taken to reflux for 4 days. The hot solution is poured into 200 ml of water and extracted with ethyl acetate. The organic solution is dried over magnesium sulfate then evaporated to dryness.

Aufarbeitung

  1. temperatureto reflux for 4 days
  2. extractionextracted with ethyl acetate
  3. dry with materialThe organic solution is dried over magnesium sulfate
  4. customthen evaporated to dryness

Quellen und Nachweise

ORD-Eintrag
ord-e602df8abd8e4825ae7ea9a34796eb20
Quelldatensatz
uspto-grants-1987_12
Patentnummer
US04710499

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