Azobisisobutyronitrile → Bicyclo[2.2.1]hept-5-ene-2-methanol norbornene maleic anhydride

Beteiligte Stoffe

Reaktionsschritte

To 70 ml of tetrahydrofuran was added 0.05 M of norbornylene, 0.15 M of bicyclo[2.2.1]hept-5-ene-2-methanol, 0.2 M of maleic anhydride and 0.4 g of AIBN. The resulting solution was reacted at 67° C. for 8 hours. Thereafter, a polymer was precipitated and filtered in petroleum ether/ether (1/1) solution, to obtain the title polymer (yield: 57%).

Herkunft & Nachweise