HRID986894
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
To 70 ml of tetrahydrofuran was added 0.05 M of norbornylene, 0.15 M of bicyclo[2.2.1]hept-5-ene-2-methanol, 0.2 M of maleic anhydride and 0.4 g of AIBN. The resulting solution was reacted at 67° C. for 8 hours. Thereafter, a polymer was precipitated and filtered in petroleum ether/ether (1/1) solution, to obtain the title polymer (yield: 57%).
WORKUP
后处理
- customThe resulting solution was reacted at 67° C. for 8 hours
- customThereafter, a polymer was precipitated
- filtrationfiltered in petroleum ether/ether (1/1) solution