1,1-Dimethylhydrazine → 2-(4-Methylvaleryl)furan dimethylhydrazone
Reaction equation
[CH3:1][CH:2]([CH3:12])[CH2:3][CH2:4][C:5]([C:7]1[O:8][CH:9]=[CH:10][CH:11]=1)=O.[CH3:13][N:14]([CH3:16])[NH2:15]>CCO>[CH3:13][N:14]([CH3:16])[N:15]=[C:5]([C:7]1[O:8][CH:9]=[CH:10][CH:11]=1)[CH2:4][CH2:3][CH:2]([CH3:12])[CH3:1]Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Procedure
A solution of 2-(4-methylvaleryl)furan (1 mmol) and N,N-dimethylhydrazine (1.5 mmol) in EtOH was heated at reflux for 24 h. Evaporation and distilation gave 2-(4-methylvaleryl)furan dimethylhydrazone as a brown oil.
Workup
- temperatureat reflux for 24 h
- customEvaporation and distilation
Sources & evidence
- ORD record
- ord-5c43bbb87c0c410f80aa0de17ced7569
- Source dataset
- uspto-grants-2000_04
- Patent number
- US06054587
Reaction notes
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