Hydrochloric Acid → HCID 178432174, compound
Reaction equation
[OH-].[Na+].C([NH:6][C:7]1[C:12]([NH:13][C:14](=O)[CH3:15])=[CH:11][CH:10]=[CH:9][C:8]=1[OH:17])(=O)C.Cl>>[OH:17][C:8]1[C:7]2[NH:6][C:14]([CH3:15])=[N:13][C:12]=2[CH:11]=[CH:10][CH:9]=1Participants
4
Procedure
To a solution of 6.8M NaOH 15.8 g (0.076 mol) of 2,3-diacetamidophenol was added and the mixture was heated under reflux for 2 h. Upon cooling the pH of the solution was adjusted to 8.5 with 2M HCl. The solid was filtered off, washed with water and dried to give 7.6 g of the title compound.
Workup
- temperaturethe mixture was heated
- temperatureunder reflux for 2 h
- temperatureUpon cooling the pH of the solution
- filtrationThe solid was filtered off
- washwashed with water
- customdried
Sources & evidence
- ORD record
- ord-b4eb2b11365742b282b0d74e02c790dd
- Source dataset
- uspto-grants-1992_04
- Patent number
- US05106862
Reaction notes
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