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Hydrochloric Acid → Methyl Ferulate

HRID 1034116
Notes
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Reaction equation

HRID 1034116 reaction equation
[C:1]([OH:14])(=[O:13])/[CH:2]=[CH:3]/[C:4]1[CH:12]=[CH:11][C:9]([OH:10])=[C:6]([O:7][CH3:8])[CH:5]=1.[N+](=[CH2:17])=[N-].Cl>CO>[C:1]([O:14][CH3:17])(=[O:13])/[CH:2]=[CH:3]/[C:4]1[CH:12]=[CH:11][C:9]([OH:10])=[C:6]([O:7][CH3:8])[CH:5]=1
ParticipantsProcedureSources & evidenceReaction notes

Participants

5

Reactant 3

HCID 313Hydrochloric AcidHCID 9550DiazomethaneHCID 445858Ferulic Acid

Product 1

HCID 5357283Methyl Ferulate

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

Methyl ferulate was prepared by methylating commercial ferulic acid (made by Tokyo Kasei Kogyo Co. LTD., Japan) with diazomethane or methyl alcohol acidified with hydrochloric acid (Fisher Method).

Sources & evidence

ORD record
ord-ae50c27527f54f52a1b67555964273d5
Source dataset
uspto-grants-1994_05
DOI
10.6084/m9.figshare.5104873.v1
Patent number
US05314693

Reaction notes

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On this pageParticipantsProcedureSources & evidenceReaction notes