Benzene → Oxazolidine, 2,2,4,4-tetramethyl-
Reaction equation
[NH2:1][C:2]([CH3:6])([CH3:5])[CH2:3][OH:4].[CH:7]1[CH:12]=CC=C[CH:8]=1>CC(C)=O>[CH3:8][C:7]1([CH3:12])[NH:1][C:2]([CH3:6])([CH3:5])[CH2:3][O:4]1Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Procedure
Firstly, the precursor compound (2,2,4,4-tetramethyl-1,3-oxazolidine was prepared. To 237 g (3.0 mole) of 2-amino-2-methyl-1-propanol, there was added approximately 750 ml of dry benzene containing 174 g (3.0 mole) of acetone.
Sources & evidence
- ORD record
- ord-96d072cfc7b34700adec4ac6bc53321a
- Source dataset
- uspto-grants-1976_05
- Patent number
- US03954985
Reaction notes
Loading…