Reaction equation
Cl.[Cl:2][C:3]1[CH:9]=[CH:8][CH:7]=[CH:6][C:4]=1[NH2:5]>C(O)C>[ClH:2].[Cl:2][C:3]1[CH:9]=[CH:8][CH:7]=[CH:6][C:4]=1[NH2:5]Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Procedure
Hydrogen chloride (HCl (gas)) was slowly bubbled through a cold (0° C.) solution of 2-chloroaniline (4.10 ml, 39 mmol) in 50 ml of ethanol (EtOH), resulting in the formation of a white precipitate which was isolated by filtration.
Workup
- customresulting in the formation of a white precipitate which
- customwas isolated by filtration
Sources & evidence
- ORD record
- ord-95eac4ac07f64299ba8147e79572ef84
- Source dataset
- uspto-grants-2000_05
- Patent number
- US06060484
Linked notes
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