Reaction equation
[C:1]1([C:3](=[CH:5][C:6](=[C:8]([CH:10]=1)[CH3:9])[CH3:7])[CH3:4])[CH3:2]>C1C=CC=CC=1>[CH:1]1[CH:3]=[CH:5][CH:6]=[CH:8][CH:10]=1.[C:1]1([C:3](=[CH:5][C:6](=[C:8]([CH:10]=1)[CH3:9])[CH3:7])[CH3:4])[CH3:2]Participants
3
Reactant 1
Product 1
Reagents, catalysts & solvents 1
Procedure
Durene was dissolved in benzene to give a molar ratio of benzene/durene of 2.2. The solution was pumped into the micro-reactor and loaded with 0.50 g of the same Fe-Mo-DBH catalyst used in Example 29 and oxidized in a flow of premixed gas consisting of 6 vol % O2 and 6 vol % N2 in He at two different temperatures, 425° C. and 450° C. Product effluent was analyzed by GC, and each product identified with GC/MS. Results are summarized in Table 23 below
Sources & evidence
- ORD record
- ord-86b9b1dd240b4b049a21ded03aa8d54a
- Source dataset
- uspto-grants-1994_06
- Patent number
- US05324702
Linked notes
Loading…