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Magnesium Chloride → HCID 178525631, compound

HRID 1157099
Notes
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Reaction equation

HRID 1157099 reaction equation
[Cl-].[Mg+2:2].[Cl-].[C:4]([OH:10])(=[O:9])[CH2:5][C:6]([OH:8])=[O:7].[CH2:11]([K])[CH3:12]>C(O)(C)C>[C:4]([O-:10])(=[O:9])[CH2:5][C:6]([O-:8])=[O:7].[CH2:11]([Mg+2:2])[CH3:12]
ParticipantsProcedureWorkupSources & evidenceReaction notes

Participants

4

Reactant 2

HCID 5360315Magnesium ChlorideHCID 178461627HCID 178461627, compound

Product 1

HCID 178525631HCID 178525631, compound

Reagents, catalysts & solvents 1

HCID 3776IsopropanolSolvent

Procedure

To a stirred aqueous solution of 1.5 M magnesium chloride and 3 M ethyl potassium malonate was added five volumes of isopropanol. After filtration, ethyl magnesium malonate was dried in vacuo.

Workup

  1. filtrationAfter filtration, ethyl magnesium malonate
  2. customwas dried in vacuo

Sources & evidence

ORD record
ord-5cf621ddc1e5409aaf773564e97814a5
Source dataset
uspto-grants-2010_10
DOI
10.6084/m9.figshare.5104873.v1
Patent number
US07807411B2

Reaction notes

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On this pageParticipantsProcedureWorkupSources & evidenceReaction notes