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TBAF tetrahydrofuran → 2-Bromo-1-[3-hydroxy-2-(tetrahydropyran-2-yloxy)propyl]-4-nitroimidazole

HRID 1158312
Notes
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Reaction equation

HRID 1158312 reaction equation
[Br:1][C:2]1[N:3]([CH2:10][CH:11]([O:21][CH:22]2[CH2:27][CH2:26][CH2:25][CH2:24][O:23]2)[CH2:12][O:13][Si](C(C)(C)C)(C)C)[CH:4]=[C:5]([N+:7]([O-:9])=[O:8])[N:6]=1.O1CCCC1.[F-].C([N+](CCCC)(CCCC)CCCC)CCC>O1CCCC1>[Br:1][C:2]1[N:3]([CH2:10][CH:11]([O:21][CH:22]2[CH2:27][CH2:26][CH2:25][CH2:24][O:23]2)[CH2:12][OH:13])[CH:4]=[C:5]([N+:7]([O-:9])=[O:8])[N:6]=1
ParticipantsProcedureWorkupSources & evidenceReaction notes

Participants

4

Reactant 2

HCID 11078149TBAF tetrahydrofuranHCID 230802502-Bromo-1-[3-(t-butyldimethylsilanyloxy)-2-(tetrahydropyran-2-yloxy)propyl]-4-nitroimidazole

Product 1

HCID 230802492-Bromo-1-[3-hydroxy-2-(tetrahydropyran-2-yloxy)propyl]-4-nitroimidazoleYield 89%

Reagents, catalysts & solvents 1

HCID 8028TetrahydrofuranSolvent

Procedure

To tetrahydrofuran (120 ml) solution of 2-bromo-1-[3-(t-butyldimethylsilanyloxy)-2-(tetrahydropyran-2-yloxy)propyl)-4-nitroimidazole (12.7 g) prepared in Example 28, was added 1M tetra-n-butylammonium fluoride tetrahydrofuran solution (30 ml) under stirring and ice-cooling condition, the reaction mixture was stirred at a room temperature overnight. The reaction mixture was concentrated under a reduced pressure and the residue was diluted with ethyl acetate, washed with water and an aqueous solution being saturated with sodium chloride. After being dried over anhydrous magnesium sulfate, the residue was concentrated under a reduced pressure, thus obtained residue was purified by use of a silica gel column chromatography (eluent: dichloromethane/ethyl acetate=10/1), there was obtained 2-bromo-1-[3-hydroxy-2-(tetrahydropyran-2-yloxy)propyl]-4-nitroimidazole (8.51 g, yield: 89%) as colorless liquid product.

Workup

  1. temperatureice-cooling condition
  2. stirringthe reaction mixture was stirred at a room temperature overnight
  3. concentrationThe reaction mixture was concentrated under a reduced pressure
  4. additionthe residue was diluted with ethyl acetate
  5. washwashed with water
  6. dry with materialAfter being dried over anhydrous magnesium sulfate
  7. concentrationthe residue was concentrated under a reduced pressure, thus obtained residue
  8. customwas purified by use of a silica gel column chromatography (eluent: dichloromethane/ethyl acetate=10/1)

Sources & evidence

ORD record
ord-99655074f19e49b9980fd121d3654b9d
Source dataset
uspto-grants-2010_10
DOI
10.6084/m9.figshare.5104873.v1
Patent number
US07807843B2

Reaction notes

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On this pageParticipantsProcedureWorkupSources & evidenceReaction notes