Trifluoroacetic acid → Sodium trihydrido(trifluoroacetato-kappaO)borate(1-)

Reaction equation

[F:1][C:2]([F:7])([F:6])[C:3]([OH:5])=[O:4].[BH4-:8].[Na+:9]>>[F:1][C:2]([F:7])([F:6])[C:3]([O:5][BH3-:8])=[O:4].[Na+:9]

Participants

Reactant 2

HCID 6422Trifluoroacetic acid

HCID 4311764Sodium borohydride

Product 1

HCID 23670384Sodium trihydrido(trifluoroacetato-kappaO)borate(1-)

Procedure

Sodium trifluoroacetoxyborohydride was prepared in situ from trifluroacetic acid and sodium borohydride, which means the operation was carried out in a single pot.

Sources & evidence

ORD record: ord-5c354f1d03f04bfb986812d6200da42f
Source dataset: uspto-grants-2014_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08664417B2

Reaction notes

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