Hydrochloric Acid → HCID 67876499, compound

Reaction equation

[N:1]1[CH:6]=[CH:5][C:4]([CH2:7][CH2:8][CH2:9][N:10]([CH2:12][CH2:13][C:14]([O:16]CC)=[O:15])[CH3:11])=[CH:3][CH:2]=1.[ClH:19]>>[ClH:19].[N:1]1[CH:6]=[CH:5][C:4]([CH2:7][CH2:8][CH2:9][N:10]([CH2:12][CH2:13][C:14]([OH:16])=[O:15])[CH3:11])=[CH:3][CH:2]=1

Participants

Reactant 2

HCID 313Hydrochloric Acid

HCID 19776451Ethyl 3-{N-[3-(pyrid-4-yl)propyl]-N-methyl-amino}-propionate

Product 1

HCID 67876499HCID 67876499, compound

Procedure

The ethyl 3-{N-[3-(pyrid-4-yl)propyl]-N-methyl-amino}-propionate obtained is refluxed for 24 hours with 600 ml of 4-n hydrochloric acid. The reaction mixture is evaporated to complete dryness, and the crystalline residue formed is separated, washed with water and dried yielding 3-{N-[3-(pyrid-4-yl)propyl]-N-methyl-amino}-propionic acid hydrochloride.

Workup

customThe reaction mixture is evaporated
customthe crystalline residue formed
customis separated
washwashed with water
customdried

Sources & evidence

ORD record: ord-eb3357b9c6914792bde6dcead5867683
Source dataset: uspto-grants-1992_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05110807

Reaction notes

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