Carbon Disulfide → HCID 178507537, compound

HRID 1241905

Reaction equation

HRID 1241905 reaction equation
[NH2:1][C:2]1[CH:3]=[C:4]([CH:9]=[CH:10][CH:11]=1)[C:5]([NH:7][NH2:8])=[O:6].C(N(CC)CC)C.[C:19](=S)=[S:20]>C(O)C>[NH2:1][C:2]1[CH:3]=[C:4]([C:5]2[O:6][C:19]([SH:20])=[N:8][N:7]=2)[CH:9]=[CH:10][CH:11]=1

Participants

5

Reactant 3

HCID 6348Carbon DisulfideHCID 8471TriethylamineHCID 84178m-Aminobenzohydrazide

Product 1

HCID 178507537HCID 178507537, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

3-Aminobenzhydrazide (5.76 g) was dissolved in ethanol (40 mL), and triethylamine (4.8 mL) and carbon disulfide (2.1 mL) were added to the solution. The mixture was heated under reflux for 4 hrs. The solvent was evaporated, and water was added. The precipitated solids were collected by filtration to give the title compound (5.06 g) as a pale-yellow powder.

Workup

  1. temperatureThe mixture was heated
  2. temperatureunder reflux for 4 hrs
  3. customThe solvent was evaporated
  4. additionwater was added
  5. filtrationThe precipitated solids were collected by filtration

Sources & evidence

ORD record
ord-2272d54bcda141169e47c2ffb68a7bea
Source dataset
uspto-grants-2006_10
Patent number
US07115635B2

Linked notes

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