Azobisisobutyronitrile → Maleic anhydride decene

HRID 1256871

Reaction equation

HRID 1256871 reaction equation
[CH3:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH:9]=[CH2:10].[C:11]1(=[O:17])[O:16][C:14](=[O:15])[CH:13]=[CH:12]1.N(C(C)(C)C#N)=NC(C)(C)C#N>C1(C)C=CC=CC=1>[C:14]1(=[O:15])[O:16][C:11](=[O:17])[CH:12]=[CH:13]1.[CH3:10][CH2:9][CH2:8][CH2:7][CH2:6][CH2:5][CH2:4][CH2:3][CH:2]=[CH2:1]

Participants

5

Reactant 3

HCID 6547AzobisisobutyronitrileHCID 7923Maleic AnhydrideHCID 133811-Decene

Product 1

HCID 22121024Maleic anhydride decene

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

Decene-1 23.0 g and maleic anhydride 15.7 g were added thereto and dissolved. Toluene 30 ml dissolving azobisisobutyronitrile 1 g was added in 3 hours. After adding, they were reacted at the same temperature for 4 hours.

Workup

  1. dissolutiondissolved
  2. additionwas added in 3 hours
  3. additionAfter adding
  4. customthey were reacted at the same temperature for 4 hours

Sources & evidence

ORD record
ord-7c0c67983010418a806158354048a921
Source dataset
uspto-grants-2013_06
Patent number
US08461271B2

Linked notes

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