3-Chloro-2,6-diethylaniline → HCID 18430566, compound
Reaction equation
[CH3:1][N:2]1[C:6]2=[N:7][C:8]3[C:14](=[O:15])[O:13][C:11](=[O:12])[C:9]=3[CH:10]=[C:5]2[CH:4]=[N:3]1.[Cl:16][C:17]1[C:18]([CH2:26][CH3:27])=[C:19]([C:21]([CH2:24][CH3:25])=[CH:22][CH:23]=1)[NH2:20]>O1CCCC1>[Cl:16][C:17]1[C:18]([CH2:26][CH3:27])=[C:19]([NH:20][C:14]([C:8]2[N:7]=[C:6]3[N:2]([CH3:1])[N:3]=[CH:4][C:5]3=[CH:10][C:9]=2[C:11]([OH:13])=[O:12])=[O:15])[C:21]([CH2:24][CH3:25])=[CH:22][CH:23]=1Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Procedure
In 100 ml of tetrahydrofuran was dissolved 8.0 g (39.4 mmol) of 1-methyl-pyrazolo[5,4-b]pyridine-5,6-dicarboxylic acid anhydride. After adding 7.23 g (39.4 mmol) of 3-chloro-2,6-diethylaniline to the solution obtained above, a reaction was carried out at ambient temperature for 12 hours.