Ethylene carbonate → HCID 18186793, compound
Reaction equation
[CH3:1][O:2][C:3]1[CH:4]=[C:5]2[C:10](=[CH:11][CH:12]=1)[CH:9]=[C:8]([OH:13])[CH:7]=[CH:6]2.C1(=O)O[CH2:17][CH2:16][O:15]1>CO.C(Cl)(Cl)Cl.CCCCCC>[CH3:1][O:2][C:3]1[CH:4]=[C:5]2[C:10](=[CH:11][CH:12]=1)[CH:9]=[C:8]([O:13][CH2:17][CH2:16][OH:15])[CH:7]=[CH:6]2Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Procedure
*Prepared from 6-methoxy-2-naphthol and ethylene carbonat according to the procedure of Example 134, step 1, in WO 00/76984. The reaction mixture was refluxed for 2 h. Pure 2-(6-methoxy-naphthalen-2-yloxy)ethanol was obtained by recrystallization from MeOH/CHCl3/n-hexane.
Workup
- temperatureThe reaction mixture was refluxed for 2 h
Sources & evidence
- ORD record
- ord-414f885c9df546a7866e1c4dbb3a2be7
- Source dataset
- uspto-grants-2003_07
- Patent number
- US06593330B2
Reaction notes
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