Reaction equation
[F:1][C:2]1[CH:7]=[C:6]([F:8])[CH:5]=[CH:4][C:3]=1[CH3:9].[Br:10]Br>[Fe]>[Br:10][C:3]1([CH3:9])[CH:4]=[CH:5][C:6]([F:8])=[CH:7][CH:2]1[F:1]Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Procedure
The title compound was prepared by a modification of a published procedure. 2,4-Difluorotoluene was treated with iron chip and bromine at 60° C. overnight under an argon atmosphere in quantitative yield.
Sources & evidence
- ORD record
- ord-2918eae845ab4176a7e95a7590c6dd31
- Source dataset
- uspto-grants-2011_02
- Patent number
- US07893224B2
Linked notes
Loading…