Potassium Carbonate → HCID 22916432, compound

HRID 1376385

Reaction equation

HRID 1376385 reaction equation
[C:1]1([C:7]2[N:8]=[N:9][NH:10][C:11]=2[C:12]2[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.Br[CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][OH:28].C(=O)([O-])[O-].[K+].[K+]>CC(=O)CC>[OH:28][CH2:27][CH2:26][CH2:25][CH2:24][CH2:23][CH2:22][CH2:21][CH2:20][CH2:19][N:9]1[N:8]=[C:7]([C:1]2[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=2)[C:11]([C:12]2[CH:13]=[CH:14][CH:15]=[CH:16][CH:17]=2)=[N:10]1

Participants

5

Reactant 3

HCID 11430Potassium CarbonateHCID 1087001-Nonanol, 9-bromo-HCID 178420171HCID 178420171, compound

Product 1

HCID 22916432HCID 22916432, compound

Reagents, catalysts & solvents 1

HCID 6569Methyl Ethyl KetoneSolvent

Procedure

4,5-Diphenyl-1,2,3-triazole was treated with 9-bromononan-1-ol and potassium carbonate in butanone to give after chromatography the title compound as a light brown oil. Found: C, 76.0; H, 8.2; N, 11.2% C23H29N30 requires: C, 76.0; H, 8.0; N, 11.6%.

Sources & evidence

ORD record
ord-d4ff176d705c4186b9cdd8687fb17aba
Source dataset
uspto-grants-1997_09
Patent number
US05663053

Linked notes

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