Trimethylsilyl cyanide → HCID 21862743, compound
Reaction equation
[CH2:1]([O:3][C:4]1[CH:21]=[CH:20][C:7]([CH:8]=[N:9][C:10]2[CH:15]=[CH:14][C:13]([S:16](=[O:19])(=[O:18])[NH2:17])=[CH:12][CH:11]=2)=[CH:6][CH:5]=1)[CH3:2].C[Si]([C:26]#[N:27])(C)C>>[CH2:1]([O:3][C:4]1[CH:21]=[CH:20][C:7]([CH:8]([NH:9][C:10]2[CH:15]=[CH:14][C:13]([S:16](=[O:19])(=[O:18])[NH2:17])=[CH:12][CH:11]=2)[C:26]#[N:27])=[CH:6][CH:5]=1)[CH3:2]Participants
3
Procedure
Following a procedure similar to that described in Example 1(ii), but using N-(4-ethoxybenzylidene)-4-sulfamoylaniline [prepared as described in step (i) above] and trimethylsilyl cyanide as starting materials, the title compound was obtained as a slightly yellow powder (yield 88%).
Sources & evidence
- ORD record
- ord-c52a00b7c75a4f529c60b8c0afb6b30e
- Source dataset
- uspto-grants-1999_06
- Patent number
- US05908858