HomeMCPWorkbenchSkills
HomeWorkbenchNotificationsMe
llms.txt · MCP GuidePrivacy Policy · Terms of Service · Supportv1.8.0
  1. Home
  2. /Reaction

Hydrogen Peroxide → HCID 14455327, compound

HRID 1420125
Notes
Print preview

Reaction equation

HRID 1420125 reaction equation
[C:1]([NH:6][C@@H:7]([C:10]([OH:12])=[O:11])[CH2:8][SH:9])(=[O:5])[CH:2]([CH3:4])[CH3:3].OO>CO>[CH3:3][CH:2]([CH3:4])[C:1]([NH:6][C@H:7]([CH2:8][S:9][S:9][CH2:8][C@@H:7]([NH:6][C:1](=[O:5])[CH:2]([CH3:3])[CH3:4])[C:10]([OH:12])=[O:11])[C:10]([OH:12])=[O:11])=[O:5]
ParticipantsProcedureWorkupSources & evidenceReaction notes

Participants

4

Reactant 2

HCID 784Hydrogen PeroxideHCID 853428N-Isobutyryl-D-cysteine

Product 1

HCID 14455327HCID 14455327, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

N-isobutyryl-D-cysteine (1 g, 5.2 mmol) was dissolved in 10 ml of methanol. Hydrogen peroxide (30%, 0.3 ml, 2.6 mmol) was added and the reaction mixture was stirred at room temperature for 6 hours. After evaporation of the solvent under reduced pressure, a white crystallised oil was obtained. Recrystallisation from ethyl acetate furnished the title compound as a white solid which was dried in vacuo.

Workup

On this pageParticipantsProcedureWorkupSources & evidenceReaction notes
  • customAfter evaporation of the solvent under reduced pressure
  • customa white crystallised oil
  • customwas obtained
  • customRecrystallisation from ethyl acetate
  • Sources & evidence

    ORD record
    ord-5ee1a527e2cd446a984390c5fca9ee42
    Source dataset
    uspto-grants-1999_03
    DOI
    10.6084/m9.figshare.5104873.v1
    Patent number
    US05889050

    Reaction notes

    Loading…