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HCID 43400514, compound → N,N-Diethyl-7-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-indole-2-carboxamide

HRID 1490576
Notes
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Reaction equation

HRID 1490576 reaction equation
CCN(CC)C(=O)c1cc2ccccc2[nH]1>C1=CCCC=CCC1.C1=CCCC=CCC1.CC(C)(C)c1ccnc(-c2cc(C(C)(C)C)ccn2)c1.CC1(C)OB(B2OC(C)(C)C(C)(C)O2)OC1(C)C.CCCCCC.C[OH2+].C[OH2+].[Ir].[Ir]>CCN(CC)C(=O)c1cc2cccc(B3OC(C)(C)C(C)(C)O3)c2[nH]1
ParticipantsConditionsSources & evidenceReaction notes

Participants

6

Reactant 1

HCID 43400514HCID 43400514, compound

Product 1

HCID 53431522N,N-Diethyl-7-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-indole-2-carboxamideYield 90%

Reagents, catalysts & solvents 4

HCID 2733548Bis(pinacolato)diboraneReagentHCID 42491874,4'-Di-tert-butyl-2,2'-bipyridylReagentHCID 76001521Bis(1,5-cyclooctadiene)dimethoxydiiridiumCatalystHCID 8058HexaneSolvent

Conditions

Temperature
60 °C

Sources & evidence

ORD record
ord-8e293438cb1946efb108f5c9265218da
Source dataset
Borylation dataset from Roche
DOI
10.1021/ja0631652

Reaction notes

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On this pageParticipantsConditionsSources & evidenceReaction notes