Benzoylhydrazine → HCID 178495846, compound

Reaction equation

[CH3:1][O:2][C:3]1[CH:11]=[C:10]2[C:6]([C:7](=O)[C:8](=[O:16])[N:9]2[CH2:12][CH2:13][O:14][CH3:15])=[CH:5][CH:4]=1.[C:18]([NH:26][NH2:27])(=[O:25])[C:19]1[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1>>[CH3:1][O:2][C:3]1[CH:11]=[C:10]2[C:6](/[C:7](=[N:27]/[NH:26][C:18](=[O:25])[C:19]3[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=3)/[C:8](=[O:16])[N:9]2[CH2:12][CH2:13][O:14][CH3:15])=[CH:5][CH:4]=1

Participants

Reactant 2

HCID 11955Benzoylhydrazine

HCID 25194459HCID 25194459, compound

Product 1

HCID 178495846HCID 178495846, compound

Procedure

The title compound was prepared as a yellow solid, using 6-methoxy-1-(2-methoxyethyl)-isatin and benzhydrazide according to the synthetic method NMR (CDCl3): δ 3.35 (s, 3H), 3.65 (t, 2H), 3.87 (s, 3H), 3.94 (t, 2H), 6.64 (d, 1H), 7.58 (t, 1H), 7.79 (d, 1H), 13.93 (br s, 1H).

Sources & evidence

ORD record: ord-3c4374304491452f8a1e3db73dd2a9ee
Source dataset: uspto-grants-2015_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US09079854B2

Reaction notes

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