Dimethylcarbamoyl Chloride → (5-(4-Chlorophenylsulfonyl)-4,5,6,7-tetrahydro-1H-pyrazolo[4,3-c]pyridin-4-yl)methyl dimethylcarbamate
Reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([S:8]([N:11]2[CH2:16][CH2:15][C:14]3[NH:17][N:18]=[CH:19][C:13]=3[CH:12]2[CH2:20][OH:21])(=[O:10])=[O:9])=[CH:4][CH:3]=1.[CH3:22][N:23]([CH3:27])[C:24](Cl)=[O:25].ClC1C=CC(S(N2C(CC)CC3(OCCO3)CC2CO)(=O)=O)=CC=1>>[CH3:22][N:23]([CH3:27])[C:24](=[O:25])[O:21][CH2:20][CH:12]1[C:13]2[CH:19]=[N:18][NH:17][C:14]=2[CH2:15][CH2:16][N:11]1[S:8]([C:5]1[CH:4]=[CH:3][C:2]([Cl:1])=[CH:7][CH:6]=1)(=[O:9])=[O:10]Participants
4
Reactant 3
Product 1
Procedure
Prepared by treatment of (5-(4-chlorophenylsulfonyl)-4,5,6,7-tetrahydro-1H-pyrazolo[4,3-c]pyridin-4-yl)methanol with dimethylcarbamyl chloride as described for compound 111 in Example 14.