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3-(1-Chloroethyl)pyridine → HCID 178463658, compound

HRID 1581160
Notes
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Reaction equation

HRID 1581160 reaction equation
CC(Cl)c1cccnc1.NCC1(c2cccc(C(F)(F)F)c2)CC1>CN(C)C=O.O=C([O-])[O-].[Cs+].[Cs+].[I-].[K+]>CC(NCC1(c2cccc(C(F)(F)F)c2)CC1)c1cccnc1
ParticipantsConditionsWorkupSources & evidenceReaction notes

Participants

6

Reactant 2

HCID 149329503-(1-Chloroethyl)pyridineHCID 28937888{1-[3-(Trifluoromethyl)phenyl]cyclopropyl}methanamine

Product 1

HCID 178463658HCID 178463658, compound

Reagents, catalysts & solvents 3

HCID 4875Potassium IodideReagentHCID 10796Cesium carbonateReagentHCID 6228DimethylformamideSolvent3×

Conditions

Temperature
70 °C

Workup

  1. aliquotNo procedure recorded
  2. additionDilution of the aliquot (2 uL) with DMSO (200 uL).

Sources & evidence

ORD record
ord-dda368c2125643d484b55b6cc1fd719a
Source dataset
Fig 7 data from Golden paper
DOI
10.1016/j.chempr.2024.04.001
Original link
View source

Reaction notes

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On this pageParticipantsConditionsWorkupSources & evidenceReaction notes