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1-(piperidin-3-ylmethyl)pyrrolidin-2-one → HCID 178436533, compound

HRID 1581225
Notes
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Reaction equation

HRID 1581225 reaction equation
CC(Cl)c1cccnc1.O=C1CCCN1CC1CCCNC1>CN(C)C=O.O=C([O-])[O-].[Cs+].[Cs+].[I-].[K+]>CC(c1cccnc1)N1CCCC(CN2CCCC2=O)C1
ParticipantsConditionsWorkupSources & evidenceReaction notes

Participants

6

Reactant 2

HCID 47120321-(piperidin-3-ylmethyl)pyrrolidin-2-oneHCID 149329503-(1-Chloroethyl)pyridine

Product 1

HCID 178436533HCID 178436533, compound

Reagents, catalysts & solvents 3

HCID 4875Potassium IodideReagentHCID 10796Cesium carbonateReagentHCID 6228DimethylformamideSolvent3×

Conditions

Temperature
70 °C

Workup

  1. aliquotNo procedure recorded
  2. additionDilution of the aliquot (2 uL) with DMSO (200 uL).

Sources & evidence

ORD record
ord-45288060bd5b40baabc8ac34c99c36a6
Source dataset
Fig 7 data from Golden paper
DOI
10.1016/j.chempr.2024.04.001
Original link
View source

Reaction notes

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On this pageParticipantsConditionsWorkupSources & evidenceReaction notes