Methyl 2-hydroxy-1-naphthoate → HCID 178498951, compound

HRID 1581283

Reaction equation

HRID 1581283 reaction equation
CC(Cl)c1cccnc1.COC(=O)c1c(O)ccc2ccccc12>CN(C)C=O.O=C([O-])[O-].[Cs+].[Cs+].[I-].[K+]>COC(=O)c1c(OC(C)c2cccnc2)ccc2ccccc12

Participants

6

Reactant 2

HCID 598533Methyl 2-hydroxy-1-naphthoateHCID 149329503-(1-Chloroethyl)pyridine

Product 1

HCID 178498951HCID 178498951, compound

Reagents, catalysts & solvents 3

HCID 4875Potassium IodideReagentHCID 10796Cesium carbonateReagentHCID 6228DimethylformamideSolvent3×

Conditions

Temperature
70 °C

Workup

  1. aliquotNo procedure recorded
  2. additionDilution of the aliquot (2 uL) with DMSO (200 uL).

Sources & evidence

ORD record
ord-be133bc78f534017aa41f18952485974
Source dataset
Fig 7 data from Golden paper
Original link
View source

Linked notes

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