5-Chlorobenzo[b]thiophene-3-methanol → HCID 178467645, compound

HRID 1581338Notes

Reaction equation

HRID 1581338 reaction equation
CC(Cl)c1cccnc1.OCc1csc2ccc(Cl)cc12>CN(C)C=O.O=C([O-])[O-].[Cs+].[Cs+].[I-].[K+]>CC(OCc1csc2ccc(Cl)cc12)c1cccnc1

Participants

6

Reactant 2

HCID 27761365-Chlorobenzo[b]thiophene-3-methanolHCID 149329503-(1-Chloroethyl)pyridine

Product 1

HCID 178467645HCID 178467645, compound

Reagents, catalysts & solvents 3

HCID 4875Potassium IodideReagentHCID 10796Cesium carbonateReagentHCID 6228DimethylformamideSolvent3×

Conditions

Temperature
70 °C

Workup

  1. aliquotNo procedure recorded
  2. additionDilution of the aliquot (2 uL) with DMSO (200 uL).

Sources & evidence

ORD record
ord-29861437b0cc4726aa9acffce202fd0e
Source dataset
Fig 7 data from Golden paper
Original link
View source

Reaction notes

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