(2S)-1-(4-methylbenzenesulfonyl)pyrrolidine-2-carboxylic acid → HCID 178427371, compound

HRID 1581375

Reaction equation

HRID 1581375 reaction equation
CC(Cl)c1cccnc1.Cc1ccc(S(=O)(=O)N2CCC[C@H]2C(=O)O)cc1>CN(C)C=O.O=C([O-])[O-].[Cs+].[Cs+].[I-].[K+]>Cc1ccc(S(=O)(=O)N2CCC[C@H]2C(=O)OC(C)c2cccnc2)cc1

Participants

6

Reactant 2

HCID 691957(2S)-1-(4-methylbenzenesulfonyl)pyrrolidine-2-carboxylic acidHCID 149329503-(1-Chloroethyl)pyridine

Product 1

HCID 178427371HCID 178427371, compound

Reagents, catalysts & solvents 3

HCID 4875Potassium IodideReagentHCID 10796Cesium carbonateReagentHCID 6228DimethylformamideSolvent3×

Conditions

Temperature
70 °C

Workup

  1. aliquotNo procedure recorded
  2. additionDilution of the aliquot (2 uL) with DMSO (200 uL).

Sources & evidence

ORD record
ord-f8491add1d26483fbd167ba1333de725
Source dataset
Fig 7 data from Golden paper
Original link
View source

Linked notes

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