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3-(1-Chloroethyl)pyridine → HCID 178437353, compound

HRID 1581410
Notes
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Reaction equation

HRID 1581410 reaction equation
C#CC1(C(=O)O)CCCC1.CC(Cl)c1cccnc1>CN(C)C=O.O=C([O-])[O-].[Cs+].[Cs+].[I-].[K+]>C#CC1(C(=O)OC(C)c2cccnc2)CCCC1
ParticipantsConditionsWorkupSources & evidenceReaction notes

Participants

6

Reactant 2

HCID 149329503-(1-Chloroethyl)pyridineHCID 920429751-Ethynylcyclopentane-1-carboxylic acid

Product 1

HCID 178437353HCID 178437353, compound

Reagents, catalysts & solvents 3

HCID 4875Potassium IodideReagentHCID 10796Cesium carbonateReagentHCID 6228DimethylformamideSolvent3×

Conditions

Temperature
70 °C

Workup

  1. aliquotNo procedure recorded
  2. additionDilution of the aliquot (2 uL) with DMSO (200 uL).

Sources & evidence

ORD record
ord-947502a1f4a149788068ce7a8b1162ed
Source dataset
Fig 7 data from Golden paper
DOI
10.1016/j.chempr.2024.04.001
Original link
View source

Reaction notes

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On this pageParticipantsConditionsWorkupSources & evidenceReaction notes