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5-Chloro-2-(4-morpholinyl)-4-pyrimidinecarboxylic acid → HCID 178470273, compound

HRID 1581416
Notes
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Reaction equation

HRID 1581416 reaction equation
CC(Cl)c1cccnc1.O=C(O)c1nc(N2CCOCC2)ncc1Cl>CN(C)C=O.O=C([O-])[O-].[Cs+].[Cs+].[I-].[K+]>CC(OC(=O)c1nc(N2CCOCC2)ncc1Cl)c1cccnc1
ParticipantsConditionsWorkupSources & evidenceReaction notes

Participants

6

Reactant 2

HCID 23249155-Chloro-2-(4-morpholinyl)-4-pyrimidinecarboxylic acidHCID 149329503-(1-Chloroethyl)pyridine

Product 1

HCID 178470273HCID 178470273, compound

Reagents, catalysts & solvents 3

HCID 4875Potassium IodideReagentHCID 10796Cesium carbonateReagentHCID 6228DimethylformamideSolvent3×

Conditions

Temperature
70 °C

Workup

  1. aliquotNo procedure recorded
  2. additionDilution of the aliquot (2 uL) with DMSO (200 uL).

Sources & evidence

ORD record
ord-6bb834a9a02c426da254b85d467a84d5
Source dataset
Fig 7 data from Golden paper
DOI
10.1016/j.chempr.2024.04.001
Original link
View source

Reaction notes

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On this pageParticipantsConditionsWorkupSources & evidenceReaction notes