3-(1-Chloroethyl)pyridine → HCID 178470181, compound

HRID 1581424Notes

Reaction equation

HRID 1581424 reaction equation
CC(Cl)c1cccnc1.O=C(O)c1nc(-c2ccccc2)n2c1CCCCC2>CN(C)C=O.O=C([O-])[O-].[Cs+].[Cs+].[I-].[K+]>CC(OC(=O)c1nc(-c2ccccc2)n2c1CCCCC2)c1cccnc1

Participants

6

Reactant 2

HCID 149329503-(1-Chloroethyl)pyridineHCID 253421753-phenyl-6,7,8,9-tetrahydro-5H-imidazo[1,5-a]azepine-1-carboxylic acid

Product 1

HCID 178470181HCID 178470181, compound

Reagents, catalysts & solvents 3

HCID 4875Potassium IodideReagentHCID 10796Cesium carbonateReagentHCID 6228DimethylformamideSolvent3×

Conditions

Temperature
70 °C

Workup

  1. aliquotNo procedure recorded
  2. additionDilution of the aliquot (2 uL) with DMSO (200 uL).

Sources & evidence

ORD record
ord-799588b22414499f99b1b0e0822434c4
Source dataset
Fig 7 data from Golden paper
Original link
View source

Reaction notes

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