N-Hydroxyphthalimide → O-(2-cyclopentylethyl)hydroxylamine

Reaction equation

O[N:2]1C(=O)C2=CC=CC=C2C1=O.[CH:13]1([CH2:18][CH2:19][OH:20])[CH2:17][CH2:16][CH2:15][CH2:14]1>>[CH:13]1([CH2:18][CH2:19][O:20][NH2:2])[CH2:17][CH2:16][CH2:15][CH2:14]1

Participants

Reactant 2

HCID 10665N-Hydroxyphthalimide

HCID 69833Cyclopentaneethanol

Product 1

HCID 21414855O-(2-cyclopentylethyl)hydroxylamine

Procedure

Prepared by a similar procedure as described for preparation 31. Starting materials: N-hydroxyphthalimide and 2-cyclopentylethanol (Lancaster). 13C-NMR (CDCl3) δ 75.7, 37.0, 34.6, 32.8, 25.1.

Workup

customPrepared by a similar procedure
customas described for preparation 31

Sources & evidence

ORD record: ord-774195c1bd814ea28313c0b0e90d6b08
Source dataset: uspto-grants-2011_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08034811B2

Reaction notes

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