Piperidine → HCID 23454950, compound

Reaction equation

N1CCCCC1.C(NNC1(N=C=S)C=CC=CC1)=O.[CH:20]([NH:22][NH:23][C:24]1[CH:29]=[CH:28][C:27]([NH:30][C:31]([N:33]([CH2:41][C:42]2[CH:47]=[CH:46][CH:45]=CC=2)CC2C=CC=CC=2)=[S:32])=[CH:26][CH:25]=1)=[O:21]>>[CH:20]([NH:22][NH:23][C:24]1[CH:25]=[CH:26][C:27]([NH:30][C:31]([N:33]2[CH2:41][CH2:42][CH2:47][CH2:46][CH2:45]2)=[S:32])=[CH:28][CH:29]=1)=[O:21]

Participants

Reactant 3

HCID 8082Piperidine

HCID 23454956HCID 23454956, compound

HCID 23454969HCID 23454969, compound

Product 1

HCID 23454950HCID 23454950, compound

Procedure

Piperidine (0.085 g, 0.001 mole) and 1-(2-formylhydrazino)phenyl isothiocyanate (0.19 g, 0.001 mole) were reacted according to the procedure described for NA-11 in Example 3. Yield 0.14 g (50 percent), m.p. 174°-176° C.

Sources & evidence

ORD record: ord-d1517927b4684480bfd8c48688f66189
Source dataset: uspto-grants-1981_06
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04276364

Reaction notes

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