1-Butanol → Propanoic acid, 3-(trichlorostannyl)-, butyl ester

Reaction equation

[Sn:1]([Cl:3])[Cl:2].[C:4](#N)[CH:5]=[CH2:6].[CH2:8]([OH:12])[CH2:9][CH2:10][CH3:11].[ClH:13].[OH2:14]>>[CH2:8]([O:12][C:4]([CH2:5][CH2:6][Sn:1]([Cl:13])([Cl:3])[Cl:2])=[O:14])[CH2:9][CH2:10][CH3:11]

Participants

Reactant 5

HCID 2631-Butanol

HCID 313Hydrochloric Acid

HCID 962Water

HCID 7855Acrylonitrile

HCID 24479Stannous Chloride

Product 1

HCID 109089Propanoic acid, 3-(trichlorostannyl)-, butyl ester

Procedure

A process according to claim 1, wherein tin dichloride is reacted with acrylonitrile, n-butanol, water and hydrogen chloride to give β-n-butoxycarbonylethyl tin trichloride.

Sources & evidence

ORD record: ord-f8aec7970c8a44608fc4fd76e74b1ed8
Source dataset: uspto-grants-1980_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04195029

Reaction notes

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