Nitroethane → HCID 3263891, compound

HRID 1706849

Reaction equation

[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]2[O:12][C:11]([CH:13]=O)=[CH:10][CH:9]=2)=[CH:4][CH:3]=1.N1CCCCC1.[N+:21]([CH2:24][CH3:25])([O-:23])=[O:22]>>[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]2[O:12][C:11]([CH:13]=[C:24]([N+:21]([O-:23])=[O:22])[CH3:25])=[CH:10][CH:9]=2)=[CH:4][CH:3]=1

Participants

Reactant 3

HCID 6587Nitroethane

HCID 8082Piperidine

HCID 6761845-(4-Chlorophenyl)-2-furaldehyde

Product 1

HCID 3263891HCID 3263891, compound

Procedure

A mixture of 82 g (0.4 mole) of 5-(p-chlorophenyl)-2-furaldehyde in 400 ml of nitroethane together with 4 ml of piperidine was heated at reflux for 2 hours.

Workup

temperaturewas heated
temperatureat reflux for 2 hours

Sources & evidence

ORD record: ord-6d59dc8dceaa4ae5a1db66d4b6e43768
Source dataset: uspto-grants-1980_06
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04209448

Linked notes

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